PHARMACEUTICAL CHEMISTRY-III (PHARMACEUTICAL ANALYSIS) (Theory)
Paper 5 Marks 100
The topics will be taught with
special reference to their Pharmaceutical Applications.
1. SPECTROSCOPIC
METHODS: Theory, Instrumentation and Pharmaceutical applications of the
following Spectroscopic Methods:
b. Atomic
Absorption and Emission Spectroscopy
c. Molecular
fluorescence spectroscopy
d. Flame
Photometry
e. I.R.
Spectroscopy
f.
Mass Spectroscopy
g. NMR
Spectroscopy
h. U.V./Visible
Spectroscopy
2. CHROMATOGRAPHIC
METHODS: Column Chromatography,
Thin Layer
Chromatography,
Gas Liquid
Chromatography, HPLC, LCMS,
GCMS, Capillary
Electrophoresis.
3. ELECTRO
CHEMICAL METHODS: Potentiometry, Polarography and Radiochemical
Techniques.
4. THERMAL
ANALYSIS: Differential Scanning Calorimetry, Differential Thermal
Analysis, Thermo Gravimetric Analysis.
5. OCCURENCE,
PROPERTIES, PREPARATION AND APPLICATION OF OFFICIAL INORGANIC COMPOUNDS: Aluminium Hydroxide, Ammonium Chloride,
Sodium Carbonate, Magnesium Carbonate, Lithium Carbonate, Sodium Nitrite,
Calcium Gluconate, Antimony Gluconate, Ferrous Fumarate, Ferrous Sulfate and
Silver Nitrate.
6. TITRIMETRIC
ANALYSIS: Acid-base titration,
Oxidation-reduction titration,
Argentometric titration, Complexometric titration,
Non-aqueous titration etc.
PHARMACEUTICAL CHEMISTRY-III (PHARMACEUTICAL
ANALYSIS) (Practical)
Paper 11 Marks 100
NOTE:- Practical of the subject shall be designed from time to time
on the basis of the above mentioned theoretical topics and availability of the
requirements e.g. Determination of the Purity and Composition of the unknown
drugs by using at least each of the above techniques. (Note: A minimum of 20
practicals will be conducted).
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