PHARMACEUTICAL CHEMISTRY-III complete syllabus

 

 

PHARMACEUTICAL CHEMISTRY-III (PHARMACEUTICAL ANALYSIS) (Theory)

Paper 5                                                                                                                                                                                                                                                                                                      Marks 100

 

The topics will be taught with special reference to their Pharmaceutical Applications.

 

1.       SPECTROSCOPIC METHODS: Theory, Instrumentation and Pharmaceutical applications of the following Spectroscopic Methods:

b.       Atomic Absorption and Emission Spectroscopy

c.       Molecular fluorescence spectroscopy

d.       Flame Photometry

e.       I.R. Spectroscopy

f.        Mass Spectroscopy

g.       NMR Spectroscopy

h.       U.V./Visible Spectroscopy

 

2.       CHROMATOGRAPHIC          METHODS: Column      Chromatography,        Thin     Layer

                       Chromatography,     Gas     Liquid    Chromatography,                             HPLC,          LCMS, GCMS,          Capillary

Electrophoresis.

 

3.       ELECTRO CHEMICAL METHODS: Potentiometry, Polarography and Radiochemical

Techniques.

 

4.       THERMAL ANALYSIS: Differential Scanning Calorimetry, Differential Thermal Analysis, Thermo Gravimetric Analysis.

 

5.       OCCURENCE, PROPERTIES, PREPARATION AND APPLICATION OF OFFICIAL INORGANIC COMPOUNDS: Aluminium Hydroxide, Ammonium Chloride, Sodium Carbonate, Magnesium Carbonate, Lithium Carbonate, Sodium Nitrite, Calcium Gluconate, Antimony Gluconate, Ferrous Fumarate, Ferrous Sulfate and Silver Nitrate.

 

6.       TITRIMETRIC ANALYSIS:   Acid-base        titration,      Oxidation-reduction    titration,

Argentometric titration, Complexometric titration, Non-aqueous titration etc. 

 

PHARMACEUTICAL CHEMISTRY-III (PHARMACEUTICAL ANALYSIS) (Practical)

Paper 11                                                                                                                                                                                                                                                                                                                        Marks 100

 

NOTE:- Practical of the subject shall be designed from time to time on the basis of the above mentioned theoretical topics and availability of the requirements e.g. Determination of the Purity and Composition of the unknown drugs by using at least each of the above techniques. (Note: A minimum of 20 practicals will be conducted).